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Atomic
Absorption Spectrophotometers
Infra-Red Spectrophotometers
UV/Visible Spectrophotometers
Gas Chromatographs
Dedicated Analyzers
High Performance Liquid Chromatographs
Accessories & Supplies

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Designed
to meet the requirements
for EPA - SW846, NPDES / RCRA
and 200.7 / 200.9 methods


| Part
Number: |
Description: |
|
411 |
Arsenic
Hydride Analyzer |
Detailed
Product Information
Using
the established platform
from the Buck 210 Series
AAS. The Unique Model
411 system provides high
throughput determination
of Arsenic from prepared
water and solid
waste samples using an integrated
continuous flow hydride generator
and electrically heated
quartz
tee tube for combustion of
the hydride material for
sub-PPB sensitivities in
the most compact dedicated
package.
Features
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Provides
detection limits of
500 parts per trillion
(0.5 parts per billion.) |
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•
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Enclosed,
electrically heated
quartz tee tube provides
safe reaction of hydride
generation products
to give stable, hi
energy arsenic signals. |
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•
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Fully
integrated continuous
flow hydride system
provides simple operation
with real-time sample
data. |
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•
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Can
be used with low cost
technical grade argon
or nitrogen purge gas
with complete flow
meter controls on instrument
for optimizing the
data. |
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•
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Internal
software capable of
multi-port linear and
quadratic calibration
curves with statistical
analysis of sample
data. |
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Direct
printout for 21-CFR
part 11 compliance
and optional data transfer
software for PC data
storage. |
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Easy
to operate with virtually
nothing to adjust |
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Unique
in-line Deuterium corrector
provides superior energy
compared to any other
arsenic method for
the best accuracy and
freedom from interferences |
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Toll-free
technical assistance
and on-line application
support. |
Summary
of Technology:
Typical
Arsenic analytical methods
usually involve either
the time-consuming modification
of an existing Flame AAS
to accommo-date a hydride
cell or using a
costly graphite furnace AAS
to reach low PPB levels needed
for most environmental screening
and remediation testing.
The well known hydride
generation
reaction (based on the classic
100+ year old marsh test
for
arsenic) provides the best
detection limits, since
it serves to
concentrate the arsenic and
isolate it from any sample
matrix. Tests can be performed
with excellent reliability
and throughput
using the continuous flow
method where the sample solution
is pre-mixed with the appropriate
hydrochloric sulfuric acid
matrix then
reacted with the strong sodium
Borohydride reducing agent
to create arsine (volatile
arsenic hydride) and free
hydrogen. This gas reaction
is passed
through
the quartz cell heated over
600º to form free arsenic
atoms which absorb the D2
corrected light from
the Buck hi through output
arsenic hollow cathode lamp
to produce precise sub PPB
level data in less than 60
seconds with
the push of a button.
| Detection
Limits: |
500
PPT (based on standard
peristaltic pump tubing) |
| Reaction
Cell: |
150mm
Annealed Quartz
T-Tube, sealed
Electrical Heater |
| Power
Requirements: |
110V/20A
for U.S. operation
& 220V/10A for
International |
| Dimensions: |
39"W
x 11"D x
12" H |
|
| Weight: |
60
lbs. |
|
Output: |
Printer
(parallel port)
Digital (RS-232)
and 1V Analog |
| Background
Corrections: |
In-Line
Deuterium Lamp
(automatic compensation) |
| Reaction
System: |
Peristaltic
pump with phase
separation glassware
& gas delivery
lines |
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